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The adsorption of colloidal goethite onto quartz and kaolinite substrates has been studied as a function of pH and NaCl concentration. Goethite adsorption was measured quantitatively by Fourier-transform infrared spectroscopy. The results indicate that adsorption onto both substrates is due primarily to coulombic forces; however, the pH dependence of adsorption is very different for the two substrates. This is explained by the fact that the surface charge on quartz is entirely pH-dependent, while kaolinite has surface faces which carry a permanent negative charge. Adsorption of goethite on to kaolinite increases markedly with increasing NaCl concentration, while adsorption onto quartz is relatively independent of NaCl concentration. This can be explained by the influence of NaCl concentration upon the development of surface charge on the substrates. A method is described for separating surface-bound goethite from free goethite.


A system of two-dimensional first-order equations for piezoelectric crystal plates with general symmetry and with electroded faces was recently deduced from the three-dimensional equations of linear piezoelectricity. Solutions of these equations for AT-cut plates of quartz were shown to give accurate dispersion curves without corrections, and the resonances predicted agree closely with the experimental data of Koga and Fukuyo [I. Koga and H. Fukuyo, J. Inst. Electr. Commun. Eng. Jpn. 36, 59 (1953)] and that of Nakazawa, Horiuchi, and Ito (M. Nakazawa, K. Horiuchi, and H. Ito, Proceedings of the 1990 IEEE Ultrasonics Symposium, pp. 547-555). In this article, these equations are employed to study the free as well as the forced vibrations of doubly rotated quartz plates. Solutions of straight-crested vibrational modes varying in the x1 and x3 directions of SC-cut quartz plates of infinite extent are obtained and from which dispersion curves are computed. Comparison of those dispersion curves with those from the three-dimensional equations shows that the agreement is very close without any corrections. Resonance frequencies for free vibrations and capacitance ratios for piezoelectrically forced vibrations are computed and examined for various length-to-thickness or width-to-thickness ratios of rectangular SC-cut quartz plates. The capacitance ratio as a function of forcing frequency is computed for a rectangular AT-cut quartz and compared with the experimental data of Seikimoto, Watanabe, and Nakazawa (H. Sekimoto, Y. Watanabe, and M. Nakazawa, Proceedings of the 1992 IEEE Frequency Control Symposium, pp. 532-536) and is in close agreement. 2ff7e9595c


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